Abstract
The N-(4-nitrophenyl)- N-methyl-2-aminoacetonitrile (NPAN) raw materials have been synthesized starting from N-methylanilide. Its solubility in different organic solvents was determined gravimetrically. Based on the solubility and crystalline nature of NPAN, an ideal solvent was selected for growing single-crystal NPAN crystal by the low-temperature solution growth technique. The large transparent yellow single crystals of NPAN were harvested in the size 36×8×8 mm 3 using 2-butanone as the solvent and in the size 21×15×15 mm 3 with nitromethane as the solvent. CHN microanalysis, differential scanning calorimeter (DSC), infrared (IR) spectra, and optical transmittance analysis have been performed to characterize the title compound.Second-harmonic generation (SHG) of the NPAN crystal was observed using Nd:YAG laser with a fundamental wavelength of 1064 nm.
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