Synthesis conditions of carbon nanotubes with the chemical vapor deposition method

Abstract

Chemical vapor deposition (CVD) enables the mass synthesis of high‐quality nanotubes. There is a large number of synthesis process parameters that have an influence on the type and form of the final product. The aim of the paper is the optimization of the synthesis process of multiwalled carbon nanotubes (MWCNTs) with the CVD method. Three synthesis parameters were selected (temperature, process time, and hydrogen flow rate) influencing the form and quality of the material produced. The experiments were carried out using our own approach to the conditions of carbon multiwalled nanotubes synthesis. The following research techniques were applied to examine the influence of selected parameters of the MWCNTs synthesis process: transmission electron microscopy (TEM), atomic force microscopy (AFM), scanning electron microscopy (SEM), and Raman spectroscopy