Abstract

Hydrogen insertion compounds of V 9Mo 6O 40 have been synthesized and investigated using incoherent inelastic neutron scattering (IINS) vibrational spectroscopy. IINS spectra of H xV 9Mo 6O 40 (x=7.8 and 17.5) confirm that in both phases H is present as coordinated hydroxyl groups. There is no evidence for the presence of coordinated water in contrast to the hydrogen insertion compounds of MoO 3 and V 2O 5.

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