Abstract
Two mononuclear oxidomolybdenum(VI) complexes, [MoO2(L1)(CH3OH)]·CH3OH (1) and [MoO2(L2)(CH3OH)] (2) (H2L1 = 3-hydroxynaphthalene-2-carboxylic acid (1-methyl-3-oxo-butylidene)hydrazide, H2L2 = 3-hydroxynaphthalene-2-carboxylic acid [1-(5-chloro-2-hydroxyphenyl)methylidene]hydrazide), were synthesized and characterized by elemental analysis, IR spectra, and single crystal X-ray diffraction. The Mo atom in each of the complexes is six-coordinated by the NNO donor atoms of the hydrazone ligand, one methanol O atom, and two oxo O atoms, forming an octahedral geometry.
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