Synthesis and x-ray structure of the tetranuclear butterfly iridium cluster Ir4(CO)8L[.mu.3-.eta.3-Ph2PC(H)CPh](.mu.-PPh2) (L = PCy3) and carbon-13, proton, and 13C{1H}, 1H, and 31P{1H} NMR studies of the compounds with L = CO, PCy3, and P(OMe)3, [carbon monoxide, tricyclohexylphosphine, and trimethyl phosphite

Fabrizia Grepioni,Maria Helena A Benvenutti,Maria D Vargas,Emilio Parisini,Brian E Mann,Dario Braga

doi:10.1021/om00032a017

Synthesis and x-ray structure of the tetranuclear butterfly iridium cluster Ir4(CO)8L[.mu.3-.eta.3-Ph2PC(H)CPh](.mu.-PPh2) (L = PCy3) and carbon-13, proton, and 13C{1H}, 1H, and 31P{1H} NMR studies of the compounds with L = CO, PCy3, and P(OMe)3, [carbon monoxide, tricyclohexylphosphine, and trimethyl phosphite

Fabrizia Grepioni, Maria Helena A Benvenutti + Show 4 more

https://doi.org/10.1021/om00032a017

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Journal: Organometallics	Publication Date: Aug 1, 1993
Citations: 16

#Trimethyl Phosphite #Carbon Monoxide + Show 5 more

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Abstract

Synthesis and x-ray structure of the tetranuclear butterfly iridium cluster Ir4(CO)8L[.mu.3-.eta.3-Ph2PC(H)CPh](.mu.-PPh2) (L = PCy3) and carbon-13, proton, and 13C{1H}, 1H, and 31P{1H} NMR studies of the compounds with L = CO, PCy3, and P(OMe)3, [carbon monoxide, tricyclohexylphosphine, and trimethyl phosphite

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