Abstract
The preparation of trisubstituted closo-decaboranes by reacting 1,2-boroxazoles with PhI(OAc)2 was studied. The process could be implemented in a one-pot variant proceeding from borylated iminol. The reaction products were characterized by 1H, 11B, and 13C NMR spectroscopy. The XRD structure of the compound [B10H7(1-IPh)(6,10-NHOCCH3)] was determined.
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