Abstract
The reaction of UCl4 with KO-2,6-Cl2C6H3 in tetrahydrofuran results in the preparation of the title compound. The six-coordinate complex possesses pseudo-octahedral geometry about uranium, with U-O(phenoxide) bond lengths in the range 2.161(11) to 2.178(10) A and U-O(THF) bond lengths of 2.467(10) and 2.475(11) A. This complex crystallizes in the monoclinic space group P21/n (a = 11.169(2), b = 11.588(2), c = 35.119(5) A, β = 92.11(1)°, V = 4542.2(13) A3, and Z = 4).
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