Abstract
Trinuclear complex Co3(O2CR)6(EtOH)2 (1) crystals were obtained in good yield (75%) by the exchange reaction between cobalt(II) chloride and potassium 3,5-di-tert-butylbenzoate (KO2CR) in EtOH. Complex 1 undergoes hydrolysis during recrystallization from non-anhydrous benzene to form the hexanuclear hydroxocarboxylate complex Co6(OH)2(O2CR)10(HO2CR)4 (2).
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