Abstract

AbstractThe efficient synthesis of new macrocycles — “monomers” and “dimers” — containing spiro‐1,3‐dioxane units is reported. The structure of the compounds was determined from high‐field NMR spectra, FAB and MALDI+ mass spectrometry investigations. The solid‐state molecular structures of three compounds was determined. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)

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