Abstract
Palladium(O) and platinum(O) phosphine complexes react with alkoxalyl chlorides (e.g., ClCOCO 2CH 3) to yield alkoxalyl complexes. The X-ray structure of one, transPd(Cl)(COCO 2CH 3)[P(C 6H 3) 3] 2, has been determined. Both the Pt and Pd complexes lose CO to give the corresponding alkoxycarbonyl complexes, M(Cl)(CO 2CH 3)[P(C 6H 5) 3] 2.
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