Abstract
The synthesis of (CF 3) 2AsCl 2N(SiMe 3) 2 is reported. This compound has been characterized on the basis of an X-ray analysis. It has a trigonal bipyramidal geometry with axial chlorine atoms. Variable temperature 1H- and 19F-NMR data show no observable changes. In comparison to pentacoordinated phosphorus compounds the tendency to form tetracoordinated derivatives is strongly diminished in the case of arsenic compounds.
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