Abstract
Compositions based on oxides and containing 5–20% w/w of ammonium molybdophosphate have been synthesized by means of different routes. Prepared samples have been studied using nitrogen adsorption–desorption, XRD, DTA–TG, and FTIR spectroscopy. Keggin structure is retained at incorporation of ammonium molybdophosphate into siliceous framework or its deposition on oxide surface and duration following calcinations up to 500 °C. Compositions possess porous structure from micromesoporous to mesomacroporous depending on the preparation method.
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