Abstract
AbstractThe hybrid transition metal – alkali metal compound, [Ni(H2O)6·(μ‐H2O)2·K2(phth)4(H2O)], (phth = phthalate) (1), was synthesized from nickel(II) nitrate, KOH and potassium hydrogen phthalate, and was isolated by crystallization. Single‐crystal X‐ray analysis revealed that 1 belongs to the monoclinic system, space group P21/c with a = 10.455(2) Å, b = 6.8670(14) Å, c = 29.704(6) Å, γ = 98.14(3)°, R1 = 0.0585, wR2 = 0.1503. In the title compound, [K2(phth)4]2+ units are bonded to water‐bridged Ni chains forming 2D lamellar‐like compounds.
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