Abstract

1,12-Bis-(N-naphthalamido)-4,9-bis-(2,4,6-trimethylbenzenesulfonyl)-4,9-diaza-dodecane 1 was obtained from 1,8-naphthalic anhydride on successive reactions with 3-aminopropanol, 4-methylbenzenesulfonyl chloride and 1,4-bis-(2,4,6-trimethylbenzenesulfonamido)butane. The molecular structure of 1 was investigated by X-ray crystallography, NMR, and mass spectrometry. The molecule crystallizes in the triclinic space group, $${P\bar 1}$$ . The cell parameters are a = 8.1548(12), b = 15.878(3), c = 18.005(3) A, α = 97.685(10), β = 93.260(15), and γ = 101.754(11)°. The asymmetric unit consists of the halves of two independent molecules, with Z = 2.

Full Text
Paper version not known

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.