Abstract
(R)‐3‐(2′‐hydroxyprop‐1‐yl) adenine 4 was obtained by alkylation of adenine 1 with R‐propylene carbonate 2 in the presence of pulverized sodium hydroxide in the synthetic process of tenofovir. The elucidation of the structure of 4 was confirmed by single crystal X‐ray diffraction and NMR experiments such as 1D 1H, 13C, and DEPT, as well as 2D COSY, HSQC, and HMBC spectra.
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