Abstract
A novel trinuclear NiII cluster, {[Ni(H2L)(EtOH)]2(OAc)2Ni} · 2EtOH [H4L:5,5′-Dihydroxy-2,2′-[ethylenedioxybis(nitrilomethylidyne)]diphenol], has been synthesized and structurally characterized. The X-ray crystal structure of the cluster reveals that two acetates coordinate to three nickel ions through Ni–O–C–O–Ni bridges and four μ-phenoxo oxygen atoms from two [Ni(H2L)] units also coordinate to nickel ions. Around three nickel atoms are all octahedral geometries.
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