Abstract
A new type of Knoevenagel condensate ligand derived from cinnamaldehyde and β-ketoanilide (acetoacetanilide) and some of its transition metal(II) complexes have been synthesized. The structural features have been determined from their microanalytical, magnetic susceptibility, IR, UV-Vis, 1 H NMR, ESR and mass spectral data. An octahedral geometry is assigned for the synthesized complexes. The Knoevenagel condensate β-ketoanilide acts as bidentate ligand. These complexes show lower conductance values, supporting their non-electrolytic nature. The monomeric nature of the complexes was confirmed from their magnetic susceptibility values. The cyclic voltammetric technique has been used to find out the anodic and cathodic peak potentials of the copper and nickel complexes.
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