Abstract
Sulfolanethiols, which were oxidized to 3,3′-disulfolanyl disulfide and 3,3′-bis(4-hydroxysulfolanyl) disulfide, were obtained by reaction of 3-sulfolene and 4-hydroxy-2-sulfolene with sodium hydrosulfide. Previously unknown cleavage of the sulfolanyl sulfides at the C-S bond of the sulfolane ring was observed during their oxidative chlorination and alkaline hydrolysis.
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