Abstract
Palladium(I) carbonyl chloride (PdCOCl)n has been synthesized by the effect of CO on PdCl2 in the presence of trace water. Anionic palladium(I) carbonyl chloride has been synthesized during treatment of ethanol-based or acetone-based solutions of H2PdCI4 containing small amounts of water; it has been isolated from the solution as the salt Cs2[Pd2(CO)2Cl4]. IR-spectra, X-ray diffraction patterns, and thermogravimetry data on synthesized palladium(I) carbonyl complexes are presented.
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