Synthesis and physico –chemical characteristics of complex ferriteCrNaFe2O5

Abstract

The article discusses for the first time the synthesis, radiographic and electron microscopic examination of CrNaFe2O5, synthesized using the high – temperature Sol-gel method. The phase of complex ferrites was synthesized using Sol-Gel synthesis method at high temperature. Initially, the structure of CrNaFe2O5 composite ferrite was researched by X-ray phase analysis and SEM, the syngony type, elementary cell parameters, radiographic and pycnometric densities and elemental analysis were defined: CrNaFe2O5 -а=5.0289, в= 5.0289, с=13.6938 Å , ρx-ray.= 5.327 g/sm3 , ρpycn.=5.331 g/sm3. A comparative analysis of the connection between the parameters of the Crystal cell of the initial materials and of the obtained complex ferrites was carried out. Through a scanning electron microscope, microsystems were taken from different parts of CrNaFe2O5 type crystallite, the elemental composition of crystals was analyzed, and the general type of surface layer of complex ferrite was displayed. As a result, the fact that the compound consists of a single phase, the clarity of its construction was determined by the topography and chemical composition of the compound. Consequently, it was discovered that the newly synthesized complex ferrites correspond to the formula CrNaFe2O5. The particles of the formed compounds have a large size (between 200 µm, 20.0 µm and 5 µm). The results of the element analysis show that the compound is compatible.