Abstract

All six regioisomeric monophosphates of octyl β- d-galactopyranosyl-(1→4)-2-acetamido-2-deoxy-β- d-glucopyranoside have been chemically synthesized and characterized by high-resolution 1H, 13C and 31P NMR spectroscopy. Phosphorylation causes characteristic downfield shifts of the nucleus at the substituted site in the 1H and 13C NMR signals and resulted in a unique 31P signal for each compound.

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