Abstract
A stable pentacoordinate bismuth compound ( 1 ) with a five-membered ring was synthesized. Reaction of 1 with sulfuryl chloride afforded a novel stable compound ( 4 ) with a covalent BiCl bond. The compound was useful for the synthesis of other hypervalent bismuth compounds with different BiC bonds such as 1c , and the selectivity in the chlorination of 1c was described.
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