Abstract
The crystal structure of the complex [NpO2(C10H8N2)(NCS)(H2O)2] · H2O is determined. The unit cell parameters are a= 7.406, b= 9.517, c= 11.518 A, α = 103.65°, β = 92.68°, γ = 96.53°, V= 781.6 A3, space group \(P\overline 1 \), Z= 2, ρ(calcd) = 2.257 g/cm3, R= 0.046, Rw= 0.122. The coordination polyhedron of the Np atom is a pentagonal bipyramid with two nitrogen atoms of dipyridyl, a nitrogen atom of isothiocyanate ion, two oxygen atoms of water molecules lying in the equatorial plane, and oxygen atoms of the neptunoyl group lying in the axial positions.
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