Abstract
AbstractThe tetranuclear cubane‐like complex, [NiL(EtOH)]4·0.5EtOH (1) with tridentate Schiff base ligand (H2L=2‐Hydroxymethyl‐N‐salicylideneaniline) has been synthesized and its crystal structure and spectroscopic properties have been studied. The complex consists of a tetranuclear (NiO)4 cubane core, of which four nickel(II) ions are bridged by μ3‐alkoxide group and each nickel(II) ion is coordinated to three μ3‐alkoxide oxygen atoms, one imino nitrogen atom and one phenoxide oxygen atom from Schiff base ligand, and further ligated by one EtOH molecule, completing a distorted octahedral geometry.
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