Abstract
A novel tri-nuclear nickel(II) complex, [Ni3L2(μ2-η1:η1-OAc)2(μ1-η1:η0-OAc)2] · H2O (H2L is N,N′-(2-hydroxypropane-1,3-diyl)-bis(salicylaldimine), was prepared. The complex was characterized by elemental analysis, IR spectra, and single crystal X-ray determination (CIF file CCDC no. 993163). Crystal of the complex crystallizes in the monoclinic space group P21/n. The unit cell parameters: a = 12.5602(9), b = 13.2104(10), c = 15.0329(10) A, β = 113.194(2)°, V = 2292.7(3) A3, Z = 2, R 1 = 0.0506, wR 2 = 0.1342, S = 1.067. The complex possesses crystallographic inversion center symmetry. The Ni atoms are in octahedral coordination spheres. The Ni⋯Ni distances are 3.022(1) A.
Published Version
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