Abstract
Nanocrystalline nickel titanate (NiTiO3) composite powders were prepared by the sol–gel process combined with a surfactant-assisted template method. The resulting powders were calcined at different temperatures ranging from 150°C to 750°C for 2 h in air. The results revealed that a pure hexagonal phase of NiTiO3 could be obtained at the low temperature of 750°C. The phase evolution of NiTiO3 was investigated by X-ray diffraction patterns, Fourier-transform infrared spectroscopy, and X-ray photoelectron spectroscopy. Particle size and morphology were studied by transmission electron microscopy.
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