Abstract
In the presence of ethylenediamine template agents, a layered antimony (III) phosphonate, [NH2CH2CH2NH2][Sb2{O3PCH(OH)CO2}2] (1) has been synthesized by hydrothermal reaction at 140°C and characterized by single-crystal X-ray diffraction as well as by infrared spectroscopy, elemental and thermogravimetric analysis. The structure of compound 1 comprises [SbO4E] trigonal bipyramids (E is the lone pair electrons occupying an axial position) and [O3PC] tetrahedra connected by [O3PCH(OH)CO2]3− to form a 2D layered structure with a one-dimensional channel system, and the ethylenediamine template agent is located inside the channels.
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