Abstract
To avoid radiation exposure in the use of nano zirconia in the ceramics and dentistry industries, a Technologically Enhanced Natural Radioactive Materials (TENORM)-free nano zirconia was required. The purpose of this research was to obtain an environmentally friendly TENORM-free nano zirconia prototype. TENORM-free nano zirconia synthesis consists of processing zircon sand into sodium zirconate, leaching of sodium zirconate to form zirconyl chloride solution, separation of impurities (silica, ThO2, U3O8, etc.), crystallization of zirconyl chloride, zirconyl-oxalate sol-gel formation, and calcination. The quality test of nano zirconia products was characterized by XRD, FT-IR, SEM, and Surveymeter, while the composition test was carried out by the XRF method. The results of this research obtained an environmentally friendly TENORM-free nano zirconia prototype, that has the chemical compound of ZrO2, the crystal size was 15.09 nm, the average particle size was 91.33 nm, free of radiation exposure, and its composition includes ZrO2: 96.599%, HfO2: 2.899%, and CaO: 0.303%. This synthesis can process zircon sand containing TENORM (ThO2: 0.070% and U3O8: 0.047%) into TENORM-free nano zirconia and increase the added value by increasing the zirconia content from 40.493% to 96.599%.
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