Abstract
Abstract A porous aluminum(III) metal-organic framework, [Al 8 (OH) 15 (H 2 O) 3 (btc) 3 ] n , MIL-110, has been synthesized by hydrothermal method and characterized by elemental analyses, X-ray powder diffraction (XRD) and IR spectroscopy. MIL-110 (Al) was calcinated at different temperatures under air atmosphere to prepare Al 2 O 3 and in another process MIL-110 (Al) nanoparticles were prepared by using oleic acid. The product of each step was characterized by scanning electron microscopy, X-ray powder diffraction (XRD) and energy-dispersive X-ray analysis (EDAX). This study demonstrates that the metal-organic frameworks may be suitable precursors for the simple one-pot preparation of nanoscale metal oxide materials with different and interesting morphologies.
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