Abstract
Two lithium bis(pyrazolyl)dialkylaluminates were prepared from equimolar amounts of [Li(tBu2pz)], AlR3 (R = Me, iBu) and tBu2pzH. Characterization was accomplished by microanalysis and spectroscopic methods as well as SCXRD. An important feature of these aluminates in solid state, is the presence of one Al-alkyl ··· Li agostic intramolecular interaction despite having used a coordinating solvent (THF) in the synthetic route.
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