Abstract
Binuclear platinum(II) complexes of the type [Pt2(ER)4(μ-Ph2PC≡CPPh2)2] (ER = SPr i , SBu t , SPh, SC6H4Cl-4, SC6F5, SePh) have been prepared and characterized by elemental analysis and NMR spectroscopy. A single-crystal X-ray structure determination of [Pt2(SC6 F5)4-(μ-Ph2PC≡CPPh2)2] has established the binuclear formulation with terminal thiolato groups. The platinum atoms lie in a distorted square planar environment with the sulfur and the phosphine ligands arranged in a cis fashion.
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