Abstract
Novel 6-alkylcarbamato/thiocarbamato-2,10-dichlorodibenzo [d,g][1,3,6,2]dioxathiaphosphocin 6-oxides were synthesized by cyclization of 5,5′-dichloro-2,2′-dihydroxydiphenyl sulfide with the corresponding dichlorophosphinyl carbamates/thiocarbamates that were obtained by the addition of alcohols/thiols to dichloroisocyanatophosphine oxide and were characterized by IR, 1H, 13C, 31P NMR, and mass spectral studies. A 13C NMR analysis revealed 2JPOC and 3JPOCC couplings. © 1996 John Wiley & Sons, Inc.
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