Abstract
A paramagnetic WIII alkyne complex bearing free terminal diphenylphosphino groups at the side-on coordinated alkyne was synthesized using a stepwise template strategy. This moderately stable metal supported open shell diphosphine shows an unprecedented spontaneous splitting of nitric oxide providing a WII-η2-C2{P(NH2)Ph2}{P(O)Ph2}+ complex featuring an amino phosphonium and a phosphine oxide substituent.
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