Abstract
AbstractAll the four isomers of Scobidiynediol (hepta‐4,6‐diyne‐2,3‐diol), a natural product isolated from white‐rot fungus Psathyrella scobinacea, were synthesized using either (R)‐ or (S)‐lactate as the source of chirality. The relative configurations of the diols were established by NOE experiments performed on the cyclic acetonides. The relative as well as absolute configurations of the natural Scobidiynediol was assigned as (2S,3S) through comparison of the optical rotation and 1H NMR data.
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