Abstract

Solution reaction of CuI and the ligand L((3-bpfob) [L: 1,3-bis(nicotinoyl) o-phenylenediamine] led to the formation of a novel coordination polymer [CuI(3-bpfob)]n that exhibited an unusual one-dimensional helical structure. The compound was characterized by x-ray crystallography, infrared (IR) spectroscopy, fluorescence spectrum, and thermal analyses. This compound crystallized in triclinic system, space group P-1, with cell parameters of a = 7.940(5), b = 10.187(6), c = 12.518(7) Å, α = 78.041(6)°, β = 72.821(6)°, γ = 72.821(6)°.

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