Abstract
Binary complex salts [Rh(NH3)5Cl][MCl6], where M = Re, Os, Ir, have been synthesized and characterized. X-ray diffraction analysis indicated that the salts are isostructural. According to X-ray phase analysis, the products of their thermolysis in hydrogen are monophase stoichiometric nonequilibrium solid solutions Rh0.5M0.5 (M = Re, Os, Ir). The molecular and crystal structures of [Rh(NH3)5Cl][OsCl6] were determined in an X-ray structural analysis.
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