Abstract
Nephritogenoside has been prepared by coupling of the acyl azide derivative of a N-triglycosyl dipeptide, derived from the corresponding hydrazide derivative of O-(2,3,4,6-tetra- O-acetyl-α- d-glucopyranosyl)-(1 → 6)- O-(2,3,4-tri- O-acetyl-β- d-glucopyranosyl)-(1 → 6)-2,3-di- O-benzyl-1- N-[ N-( tert-butoxycarbonyl)- l-aspart-1-oyl-( l-proline methyl ester)-4-oyl]-α- d-glucopyranosylamine, with a nonadecapeptide, followed by deprotection of the desired protected nephritogenoside. The N-triglycosyl pentapeptide also has been prepared as a model compound.
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