Abstract
Single crystals of TlCu(OH)SO 4 and TlCu(OH)SeO 4 were prepared under hydrothermal conditions. The isotypic structures were solved by direct method strategy and Fourier summations, using single crystal X-ray data up to sin θ/λ = 0.8 A #751 [space group P2 1 /m (No. 11); a = 8.854(2) A, 9.041(6) A; b = 5.888(1) A, 5.959(3) A; c = 4.493(1) A, 4.584(2) A; β = 95.29(3)°, 94.26(2)°; Z = 2; R w = 0.052, 0.043 for 924, 952 reflections]. The copper atoms are [4+2]-coordinated, the thallium atoms have an irregular seven-coordination
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