Abstract
AbstractA glycoside ester product was prepared by the transglycosylation of starch and glycerol, which yielded a mixture of 2,3‐dihydroxypropyl‐α‐D‐glucopyranoside and other glycerol glycosides, followed by interesterification of the crude glycerol glycosides with a mixture of mono‐, di‐ and tripalmitin. The purified reaction product, consisting of ca. 77% glycerol glycoside palmitates, 14% palmitins and 9% free palmitic acid, was found to be extremely effective in lowering the interfacial tension between cottonseed oil and water—a 0.04% concentration in the oil phase lowering the interfacial tension to 1.3 dynes/cm.
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