Abstract
One pot condensation of malonic acid dihydrazide (MADH) in the presence of metal salts (CuCl2·H2O and ZnCl2) with melamine (TAT) has been achieved. The solids Cu(MADH)2Cl2·2TAT·9H2O and Zn(MADH)2Cl2·TAT·1/2H2O thus obtained were characterized by elemental analysis, FAB mass, i.r., n.m.r., u.v.–visible and e.p.r. spectral data together with their powder X-ray diffraction, optical microscopy, scanning electron microscopy (SEM) and atomic force microscopy (AFM)(Zn complex only). Variable temperature solid slate conductance measurements have also been made.
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