Abstract
An environmentally viable, green and efficient protocol for the synthesis of polyhydroquinolines using sulfated polyborate catalyst have been developed by Hantzsch four-component condensation between aromatic aldehydes, dimedone, ammonium acetate and ethylacetoacetate or ethylcyanoacetate at 100 °C under solvent-free condition. The sulfated polyborate catalyst is characterized by FT-IR, XRD, SEM and EDAX techniques. The noticeable features of this methodology are mild Bronsted acidic nature of the catalyst, good to excellent product yields (85–94%), short reaction time (18–30 min), solvent-free condition, operational simplicity and applicability to a wide range of substrates (29 examples). This work deals with sulfated polyborate catalysed green and efficient solvent-free synthesis of polyhydroquinolines.
Published Version
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