Abstract
A highly selective, rapid one-step radiochemical separation procedure for palladium has been developed. It is based on the solvent extraction of palladium diethyldithiocarbamate from a 5 M hydrochloric acid solution with a substoichiometric amount of copper diethyldithiocarbamate in chloroform. The separation has been applied to the determination of traces of palladium by neutron-activation analysis, in platinum, the rocks W-1 and PCC-1 and a biological material (kale). Amounts of palladium down to 10 −8 g have been determined.
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