Abstract
This study experimentally investigated the effect of wettability and sudden changes in flow area on liquid-liquid extraction operation. The wall surface wettability has been altered by connecting the glass capillary (hydrophilic) and poly(tetrafluoroethylene) (PTFE)-coated capillary (hydrophobic) together in four different arrangements. In all of the arrangements, a 2 mm inner diameter tube of 35 cm length is used upstream, while a 1 mm inner diameter tube of 35 cm length is used downstream. Acetic acid mixed with toluene and water is used as a test fluid. Various flow patterns are observed: slug, droplet, slug with the droplet, and encapsulated drop in slug. The extraction efficiency is observed to be the maximum when the hydrophobic tube is used upstream, followed by a hydrophilic tube downstream. Due to the contraction effect, the specific surface area of the slug increases from 1.6 to 2.7 times. Further numerical simulations have been run using open CFD software OpenFoam to see the inner flow physics at the maximum efficiency due to a sudden jump in wettability. The presence of a recirculating zone downstream just after the plane of area change leads to the formation of encapsulated drop and enhances circulation within the slug.
Published Version
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