Abstract
Bisphenol S replaces bisphenol A to synthesize bisphenol S polycarbonate, which introduces the sulfone group in polycarbonate, improves the heat resistance and flame resistance of polycarbonate, and expands its application field. In this experiment, bisphenol S reacts with triphosgene to synthesize bisphenol S polycarbonate by interface polycondensation method. The effects of various factors on the product’s molecular weight are investigated and the optimal conditions of reaction are obtained. Through the infrared absorption spectrum, we verify the product structure. Through the Ubbelohde viscometer, the maximum viscosimeter molecular weight is measured and calculated to be 18500. Through the dilatometer, we detect the product’s temperature of glass transition at 166.5°C, which indicates that bisphenol S polycarbonate has good heat resistance. The limiting oxygen index of the product is 33.5%, and the combustion performance level reaches V-0, which indicates that bisphenol S polycarbonate has good flame retardancy.
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