Abstract

The isothermal compression experiment of as-rolled Ti55 alloy was carried out on a Gleeble-3800 thermal simulation test machine at the deformation temperature range of 700–1050 °C and strain rate range of 0.001–1 s−1. The hot deformation behavior and the microstructure evolution were analyzed during thermal compression. The results show that the apparent activation energy Q in α+β dual-phase region and β single-phase region were calculated to be 453.00 KJ/mol and 279.88 KJ/mol, respectively. The deformation softening mechanism was mainly controlled by dynamic recrystallization of α phase and dynamic recovery of β phase. Discontinuous yielding behavior mainly occurred in β phase region, which weakened gradually with the increase of deformation temperature (>990 °C) and strain rate (0.01–1 s−1) in β phase region. The processing map derived from Murty’s criterion was more accurate in predicting the hot workability than that derived from Prasad’s criterion. The optimized hot working window was 850–975°C/0.001–1 s−1, in which sufficient dynamic recrystallization occurred and α + β-transus microstructure was obtained. When deformed at higher temperature (≥1000 °C), coarsened lath-shape β-transus microstructure was formed, while deformed at lower temperature (≤825 °C) and higher strain rate (≥0.1 s−1), the dynamic recrystallization was not sufficient, thus flow instability appeared because of shear cracking.

Highlights

  • Ti-55 alloy is a near α titanium alloy with the nominal chemical composition Ti-(5.0–6.0)Al-(3.0–4.0)Sn-(2.5–3.3)Zr-(0.3–1.5)Mo-(0.2–0.7)Ta-(0.2–0.7)Nb-(0.1–0.5)Si, which shows high strength and excellent corrosion resistance

  • Single-phase region, which should be caused by lower deformation temperature and less slip system of α phase than β phase

  • The hot compression experiment of as-rolled Ti55 alloy was conducted in the temperature range of 700–1050 °C and strain rate range of 0.001–1 s−1

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Summary

Introduction

Ti-55 alloy is a near α titanium alloy with the nominal chemical composition Ti-(5.0–6.0)Al-(3.0–4.0)Sn-(2.5–3.3)Zr-(0.3–1.5)Mo-(0.2–0.7)Ta-(0.2–0.7)Nb-(0.1–0.5)Si (wt %), which shows high strength and excellent corrosion resistance. Similar to other high temperature titanium alloys, such as Ti-1100 and IMI834, this alloy is quite difficult to be formed into a complex shape because of its poor workability and high strength. In order to develop plastic forming methods of high temperature titanium alloys, such as forging, extrusion and sheet hot forming, it is necessary to characterize the deformation behavior, including the flow stress behavior, deformation mechanism and microstructure evolution of the materials. Quite a few investigations have been conducted to analyze the hot deformation behavior of high temperature titanium alloys. Niu et al [7] investigated the high temperature behavior of a near-α Ti-600 alloy and determined its optimized superplastic forming window

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