Study of the fusion zone and heat-affected zone microstructures in tungsten inert gas-welded INCONEL 738LC superalloy

Abstract

The fusion zone and heat-affected zone (HAZ) microstructures obtained during tungsten inert gas (TIG) welding of a commercial superalloy IN 738LC were examined. The microsegregation observed during solidification in the fusion zone indicated that while Co, Cr, and W segregated to the γ dendrites, Nb, Ti, Ta, Mo, Al, and Zr were rejected into the interdendritic liquid. Electron diffraction and energy-dispersive X-ray microanalyses using a transmission electron microscope (TEM) of secondary phases, extracted from the fusion zone on carbon replicas, and of those in thin foils prepared from the fusion zone showed that the major secondary solidification constituents, formed from the interdendritic liquid, were cubic MC-type carbides and γ-γ’ eutectic. The terminal solidification reaction product was found to consist of M3B2 and Ni7Zr2 formed in front of the interdendritic γ-γ’ eutectic. Based on the knowledge of the Ni-Ti-C ternary system, a pseudoternary solidification diagram was adapted for IN 738 superalloy, which adequately explained the as-solidified microstructure. The HAZ microfissuring was observed in regions surrounding the fusion zone. Closer and careful microstructural examination by analytical scanning electron microscopy revealed formation of re-solidified constituents along the microfissured HAZ grain boundaries, which suggest that HAZ cracking in this alloy involves liquation cracking. Liquation of various phases present in preweld alloy as well as characteristics of the intergranular liquid film contributing to the alloy’s low resistance to HAZ cracking were identified and are discussed.