Abstract

Nanocrystalline indium oxide powders were prepared by combustion synthesis. The changes of nanostructure caused by material processing were studied using X-ray powder diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and Brummer Emette teller analysis (BET). The stoichiometric composition of the starting indium tin oxide powder (cubic in traces) induced phase transitions to high temperature. We found that the phase transition to ITO was initiated at the surface of the small particles, while transition from cubic to rutile started in their center. Changes in crystallite size during annealing process were obtained by the Scherer method, while the particle size changes were monitored by TEM. The difference in the results obtained by this combustion technique was explained in frame of basic physical properties characterizing both methods. Keywords: XRD, BET, TEM, FTIR.

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.