Study of laser heated iron using third generation synchrotron X-ray radiation facility with imaging plate at high pressures

Abstract

Iron pressurized to 60 gigapascal (GPa) was heated with laser up to temperatures of over 2200 K. The structural changes were determined in-situ using third generation synchrotron X-ray source; the changes were recorded on an imaging plate with a monochromatic beam. The results strongly support the existence of a phase transformation of the hexagonal close-packed (hcp) structure to the new polymorph (β-phase of iron) at high pressure and temperature. We interpret the X-ray data as belonging to the double hexagonal close-packed (dhcp) structure distorted by stress due to laser heating.