Abstract

By means of dioxane dibromide the bromination of number of homologs of 1,6-dioxaspiro[4.4]nonane was achieved, as a result of which nine mono and dibromo-derivatives of spiranes were obtained which have not been described in the literature. It was established that bromine enters into position 4 and 9 of the 1,6-dioxaspiro[4.4]nonane ring.

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