Abstract
Palladium monothioacetylacetonate (Pd (SAA)2) was found to be converted into palladium dithioacetylacetonate (Pd (SSAA)2) in the presence of sodium sulfide. It was indicated that this reaction follows first order kinetics with respect to the concentrations of Pd (SAA)2 and sodium sulfide, respectively and on the whole, second order kinetics. A new spectrophotometric method of determination of sulfide ion, which is applicable in the range from 8 μg to 240 μg of sulfide ion, was devised by the measurement of the absorbance of Pd (SSAA)2 formed (510mμ).
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